1: 2-picoline With n-butyllithium in diethyl ether; hexane
T=-78 - 20°C;
2: dimethyl diselenide in tetrahydrofuran; diethyl ether; hexane
T=-78 - 20°C;
参考文献
Jones, Roderick C.; Canty, Allan J.; Gardiner, Michael G.; Skelton, Brian W.; Tolhurst, Vicki-Anne; White, Allan H.
Inorganica Chimica Acta, 2010 , vol. 363, # 1 p. 77 - 87
1: 2-picoline With n-butyllithium in tetrahydrofuran; hexane
T=-78°C;
2: With selenium in tetrahydrofuran; hexane
T=20°C;
3: methyl iodide in tetrahydrofuran; hexane
T=20°C; 16 h;
参考文献
Skelton, Brian W.; Tolhurst, Vicki-Anne; White, Allan H.; Williams, Alan M.; Wilson, Adele J.
Journal of Organometallic Chemistry, 2003 , vol. 674, # 1-2 p. 38 - 44