CIS-4-环己烯-1,2-二甲酸二甲酯合成路线 （共 22 条）
反应条件
Amberlyst 15 in methanol 216 h;
参考文献
Schwizer, Daniel; Patton, John T.; Cutting, Brian; Smiesko, Martin; Wagner, Beatrice; Kato, Ako; Weckerle, Celine; Binder, Florian P. C.; Rabbani, Said; Schwardt, Oliver; Magnani, John L.; Ernst, Beat
Chemistry - A European Journal, 2012 , vol. 18, # 5 p. 1342 - 1351
反应条件
toluene-4-sulfonic acid Heating;
参考文献
Finikova, Olga S.; Cheprakov, Andrei V.; Beletskaya, Irina P.; Carroll, Patrick J.; Vinogradov, Sergei A.
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 522 - 535
反应条件
Amberlystreg; 15 336 h; Amberlyst.(R). 15;
参考文献
GlycoMimetics, Inc.
Patent: US2008/161546 A1, 2008 ;
Location in patent: Page/Page column 17; title page ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in methanol T=20°C; chemoselective reaction;
参考文献
Jana, Amit Kumar; Karmakar, Raju; Dinda, Bidyut Kumar; Mitra, Prithiba; Ghosh, Ketaki; Karmakar, Rajdip; Mal, Dipakranjan
Journal of the Indian Chemical Society, 2012 , vol. 89, # 7 p. 975 - 979
反应条件
1: (CF3CO)2O 2: methanol View Scheme
参考文献
Schneider, Manfred; Engel, Norbert; Hoenicke, Petra; Heinemann, Gerd; Goerisch, Helmut
Angewandte Chemie, 1984 , vol. 96, # 1 p. 55 - 56
反应条件
toluene T=150 - 160°C;
参考文献
Petrow; Sopow
Sb. Statei Obshch. Khim., 1953 , p. 853,855
Chem.Abstr., 1955 , p. 5329
参考文献
Mohr, Peter; Waespe-Sarcevic, Nada; Tamm, Christoph; Gawronska, Krystyna; Gawronsky, Jacek K.
Helvetica Chimica Acta, 1983 , vol. 66, # 8 p. 2501 - 2511
参考文献
Nasarow; Kutscherow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1954 , p. 329,333; engl. Ausg. S. 269, 272
反应条件
(i) , (ii) /BRN= 102415/; Multistep reaction;
参考文献
Klein,J. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 935 - 939
反应条件
1.1: sodium hydroxide / water / 20 °C / pH 7 / Aqueous phosphate buffer 2.1: phosgene / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C 2.2: 3.33 h / Reflux 3.1: sodium hydroxide / water / 20 °C / pH 7 / Aqueous phosphate buffer View Scheme
参考文献
GLYCOMIMETICS, INC.; MAGNANI, John, L.; SARKAR, Arun, K.
Patent: WO2012/61662 A1, 2012 ;
