2,3-二羟基-1,4-二氧杂环己烷合成路线 （共 16 条）
反应条件
in ethanol
T=20°C; 2 h;
参考文献
MYRIAD GENETICS, INC.; CYTOVIA, INC.
Patent: WO2005/3100 A2, 2005 ;
Location in patent: Page 134; 233 ;
WO 2005/003100 A2
参考文献
Sankio Chemical Co., Ltd.
Patent: US6504032 B1, 2003 ;
反应条件
1: ethyl 2-(4-amino-3-nitrophenyl)acetate With hydrogen; palladium 10 on activated carbon in methanol
T=20°C; 6 h;
2: 2,3-dihydroxy-1,4-dioxane in methanol
T=20°C; 2 h;
参考文献
Baroni, Marco; Bourrie, Bernard; Casellas, Pierre
Patent: US2004/138264 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
1: 4-amino-3-nitrophenylacetic acid With palladium 10 on activated carbon; hydrogen in methanol
T=20°C; 6 h;
2: 2,3-dihydroxy-1,4-dioxane in methanol
T=20°C; 2 h;
参考文献
SANOFI-SYNTHELABO
Patent: JP2004/525983 A, 2004 ;
Location in patent: Page/Page column 16-17 ;
反应条件
in ethanol
T=20°C; 3 h;
参考文献
Shkurko, O. P.; Gogin, L. L.; Baram, S. G.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 2 p. 216 - 221
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 2 p. 257 - 262
反应条件
potassium cyanide; potassium carbonate in ethanol
参考文献
Venuti, Michael C.
Synthesis, 1982 , # 1 p. 61 - 63
