甲基 4-(吲哚-2-基)苯甲酸合成路线 (共 12 条)
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere 2: potassium carbonate; L-proline; copper(I) bromide / dimethyl sulfoxide / 3 h / 100 °C / Inert atmosphere View Scheme
参考文献
Ponpandian, Thanasekaran; Muthusubramanian, Shanmugam
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4248 - 4252
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 24 h / 20 - 50 °C / |Inert atmosphere; |Schlenk technique 2: Au/Carbon G-60 catalyst / toluene / 48 h / 90 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Perea-Buceta, Jesus E.; Wirtanen, Tom; Laukkanen, Otto-Ville; Maekelae, Mikko K.; Nieger, Martin; Melchionna, Michele; Huittinen, Nina; Lopez-Sanchez, Jose A.; Helaja, Juho
Angewandte Chemie - International Edition, 2013 , vol. 52, # 45 p. 11835 - 11839
Angew. Chem., 2013 , vol. 125, # 45 p. 12051 - 12055,5