反应条件
in tetrahydrofuran react. in THF, treatment of reat.-mixture with 10percent aq. NaOH, separation of upper layer, removal of THF, cooling to 0°C;; drying in vac. at 60-70°C; purity: 99.8percent;;
参考文献
Gmelin Handbook: B: B-Verb.14, 3.7.2.1, page 72 - 74
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Metal Hydrides Inc.
Patent: US3317525 , 1967 ;
C. A., 1967 , vol. 67, p. 21921