反应条件
Multi-step reaction with 2 steps 1: 1.) Sn(OSO2CF3)2, N-ethylpiperidine / 1.) THF, -5 - 0 deg C, 3-4 h 2.) THF, -5 - 0 deg C, 2 h2: 59 percent / LiAlH4 / tetrahydrofuran / 1.) 0 deg C, 5 min 2.) reflux, 2 h
参考文献
Nagao, Yoshimitsu; Dai, Wei-Min; Ochiai, Masahito; Tsukagoshi, Shigeru; Fujita, Eiichi Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 289 - 291
