4-氨基-N-(2-羟乙基)苯磺酰胺合成路线 (共 4 条)
反应条件
hydrogen; acetic acid; palladium on activated charcoal in tetrahydrofuran
P=760 Torr;
参考文献
Misra, Raj N.; Xiao, Hai-Yun; Williams, David K.; Kim, Kyoung S.; Lu, Songfeng; Keller, Kristen A.; Mulheron, Janet G.; Batorsky, Roberta; Tokarski, John S.; Sack, John S.; Kimball, S. David; Lee, Francis Y.; Webster, Kevin R.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 11 p. 2973 - 2977
参考文献
Bauer
Journal of the American Chemical Society, 1939 , vol. 61, p. 613,616
Full Text Show Details
Adams; Long; Johanson
Journal of the American Chemical Society, 1939 , vol. 61, p. 2342,2344
反应条件
1: 70 percent / Et3N / 0 - 25 °C
2: 84 percent / H2; AcOH / Pd/C / tetrahydrofuran / 760 Torr
View Scheme
参考文献
Misra, Raj N.; Xiao, Hai-Yun; Williams, David K.; Kim, Kyoung S.; Lu, Songfeng; Keller, Kristen A.; Mulheron, Janet G.; Batorsky, Roberta; Tokarski, John S.; Sack, John S.; Kimball, S. David; Lee, Francis Y.; Webster, Kevin R.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 11 p. 2973 - 2977
反应条件
2: aqueous hydrochloric acid
View Scheme
参考文献
Bauer
Journal of the American Chemical Society, 1939 , vol. 61, p. 613,616
Full Text Show Details
Adams; Long; Johanson
Journal of the American Chemical Society, 1939 , vol. 61, p. 2342,2344