二-Alpha-萘二亚胺合成路线 (共 18 条)
反应条件
zinc in methanol T=25°C; 0.15 h; Inert atmosphere;
参考文献
Han; Yu; Xu; Song; Yan; Ma; Zhen
Journal of Chemical Research, 2013 , vol. 37, # 1 p. 55 - 56
反应条件
triethylammonium formate; magnesium in methanol
T=20°C; 3 h;
参考文献
Srinivasa; Abiraj; Gowda, D. Channe
Australian Journal of Chemistry, 2004 , vol. 57, # 6 p. 609 - 610
反应条件
1-benzyl-4-aza-1-azoniabiyclolt;2.2.2gt;octane peroxodisulfate in acetonitrile
Oxidation; 0.333333 h; Heating;
参考文献
Hajipour; Mohammadpoor Baltork; Kianfar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 5 p. 607 - 610
反应条件
sodium ditelluride in tetrahydrofuran; N,N-dimethyl-formamide
T=70°C; 5 h;
参考文献
Suzuki, Hitomi; Manabe, Hajime; Kawaguchi, Takashi; Inouye, Masahiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 771 - 772
反应条件
hydrazine hydrate; nickel(II) nitrate hexahydrate; zinc in tert-butyl alcohol
0.833333 h; Heating;
参考文献
Yun, Tae Ho; Park, Moon Keu; Han, Byung Hee
Journal of Chemical Research, Miniprint, 1992 , # 10 p. 2774 - 2788
反应条件
in various solvent(s)
T=155°C; 12 h;
参考文献
Nay, Barry; Scriven, Eric F. V.; Suschitzky, Hans; Thomas, Desmond R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 611 - 613
反应条件
water; ammonium chloride; zinc in N,N-dimethyl-formamide
T=80°C; 1 h; microwave irradiation; Product distribution; Further Variations:Temperaturestime, irradiation;
参考文献
Cravotto, Giancarlo; Boffa, Luisa; Bia, Marco; Bonrath, Werner; Curini, Massimo; Heropoulos, Georgios A.
Synlett, 2006 , # 16 p. 2605 - 2608
反应条件
alkaline potassium sulfite
unter Kuehlung und laesst das erhaltene α-naphthalindiazosulfonsaure Kalium einige Tage im Exsiccator bei gewoehnlicher Temperatur stehen;
参考文献
Hantzsch; Schmiedel
Chemische Berichte, 1897 , vol. 30, p. 79
反应条件
ethanol; sulfuric acid; sodium nitrite
und faellt dann mit Wasser;
参考文献
Nietzki; Goll
Chemische Berichte, 1885 , vol. 18, p. 298
反应条件
acetic anhydride
Heating;
参考文献
Smalley,R.K.; Suschitzky,H.
Journal of the Chemical Society, 1963 , p. 5571 - 5572