1-(2,4-二羟基苯基)-2-(4-甲氧基苯基)乙酮合成路线 (共 38 条)
参考文献
Chemische Berichte, , vol. 66, p. 686
参考文献
Chemistry of Natural Compounds, , vol. 24, # 4 p. 432 - 438
Khimiya Prirodnykh Soedinenii, , vol. 24, # 4 p. 511 - 519
反应条件
sodium hydroxide; dihydrogen peroxide T=50°C; Reaktion ueber mehrere Stufen;
参考文献
Baker; Jukes; Subrahmanyam
Journal of the Chemical Society, 1934 , p. 1681,1683
反应条件
potassium carbonate in N,N-dimethyl-formamide T=115°C; 2 h;
参考文献
Matin, Azadeh; Gavande, Navnath; Kim, Moon S.; Yang, Nancy X.; Salam, Noeris K.; Hanrahan, Jane R.; Roubin, Rebecca H.; Hibbs, David E.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 21 p. 6835 - 6850
反应条件
1: With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate in acetone T=20 - 75°C; Baker-VenKataraman transformation; 12 h; 2: With potassium hydroxide in ethanol 0.333333 h; Heating; Further stages.;
参考文献
Dai, DeMing; Weng, LingLing
Journal of Chemical Research, 2007 , # 10 p. 572 - 573
反应条件
1: sodium acetate 2: ethanol; sulfuric acid View Scheme
参考文献
Wessely; Lechner
Monatshefte fuer Chemie, 1931 , vol. 57, p. 395,403
参考文献
Baker; Jukes; Subrahmanyam
Journal of the Chemical Society, 1934 , p. 1681,1683
反应条件
pyridin-2-yl hydrobromide 0.0166667 h; Heating;
参考文献
Jain, Amolak C.; Nayyar, Naresh K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 136 - 139
反应条件
1: 2.45 g / pyridinium bromide / 0.02 h / Heating 2: potassium carbonate / acetone / 30 - 35 °C 3: potassium carbonate / acetone / 1) 10-15 min, 40-50 deg C 2) 1 h, 60-70 deg C 4: 62.5 percent / 4 percent aq. sodium carbonate / ethanol / 1 h / Heating 5: 90.8 percent / 10 percent methanolic hydrochloric acid / methanol / 0.25 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, # 1-12 p. 136 - 139
反应条件
boron trifluoride diethyl etherate
T=60 - 70°C; 1.5 h;
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008