2,2’-二甲氧基联苯合成路线 （共 133 条）
反应条件
1: methoxybenzene With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; cobalt(II) dibromide in tetrahydrofuran; hexane T=0 - 20°C; 0.5 h; 2: alpha-chloropyridine in tetrahydrofuran; hexane T=50°C; 3: With water in tetrahydrofuran; hexane
参考文献
Dayaker, Gandrath; Chevallier, Floris; Gros, Philippe C.; Mongin, Florence
Tetrahedron, 2010 , vol. 66, # 46 p. 8904 - 8910
反应条件
CuI*2LiI; oxygen; phenyllithium in various solvent(s) T=-125°C; Further byproducts given. Yields of byproduct given;
参考文献
Lipshutz, Bruce H.; Kayser, Frank; Siegmann, Konstantin
Tetrahedron Letters, 1993 , vol. 34, # 42 p. 6693 - 6696
反应条件
1: in tetrahydrofuran T=20°C; 2 h; 2: With iodine in tetrahydrofuran T=0 - 60°C; 16 h;
参考文献
Nguyen, Tan Tai; Chevallier, Floris; Jouikov, Viatcheslav; Mongin, Florence
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6787 - 6790
反应条件
1: methoxybenzene With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; cobalt(II) dibromide in tetrahydrofuran; hexane T=0 - 20°C; 2 h; 2: allyl bromide in tetrahydrofuran; hexane T=20°C; 3: With water in tetrahydrofuran; hexane
参考文献
Dayaker, Gandrath; Chevallier, Floris; Gros, Philippe C.; Mongin, Florence
Tetrahedron, 2010 , vol. 66, # 46 p. 8904 - 8910
反应条件
FeCl2(N(C2H5)2CH2CH2NC(CH3)CHC(CH3)O) in diethyl ether T=20°C; 1 h; Inert atmosphere;
参考文献
Yamaguchi, Yoshitaka; Ando, Hiroaki; Nagaya, Makoto; Hinago, Hideto; Ito, Takashi; Asami, Masatoshi
Chemistry Letters, 2011 , vol. 40, # 9 p. 983 - 985
反应条件
tributylphosphine; potassium iodide; niobium bromide in N,N,N',N',N'',N''-hexamethylphosphoric triamide; N,N-dimethyl-formamide T=50°C; 1.5 h;
参考文献
Takagi, Kentaro; Hayama, Naomi; Inokawa, Saburo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 12 p. 3691 - 3695
反应条件
CoCl2 in acetonitrile T=80°C;
参考文献
Iqbal, Javed; Khan, M. A.; Nayyar, Naresh K.
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5179 - 5182
反应条件
CoCl2 in acetonitrile T=80°C;
参考文献
Iqbal, Javed; Khan, M. A.; Nayyar, Naresh K.
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5179 - 5182
反应条件
CoCl2 in acetonitrile T=80°C;
参考文献
Iqbal, Javed; Khan, M. A.; Nayyar, Naresh K.
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5179 - 5182
反应条件
[2,2']bipyridinyl; NiBr2bipy in various solvent(s) T=20°C; electrochemical reaction, magnesium anode, gold gauze cathode, -1,2 V; Yield given. Yields of byproduct given;
参考文献
Rollin, Yolande; Troupel, Michel; Tuck, Dennis G.; Perichon, Jacques
Journal of Organometallic Chemistry, 1986 , vol. 303, p. 131 - 138
