2,2’-二甲氧基联苯合成路线 （共 133 条）
反应条件
isoquinoline; copper
参考文献
Gilman; Swiss; Cheney
Journal of the American Chemical Society, 1940 , vol. 62, p. 1963,1965
反应条件
CuI*2LiI; oxygen in various solvent(s) T=-125°C; Yield given. Further byproducts given;
参考文献
Lipshutz, Bruce H.; Kayser, Frank; Siegmann, Konstantin
Tetrahedron Letters, 1993 , vol. 34, # 42 p. 6693 - 6696
反应条件
CoCl2 in acetonitrile T=80°C; Further byproducts given;
参考文献
Iqbal, Javed; Khan, M. A.; Nayyar, Naresh K.
Tetrahedron Letters, 1991 , vol. 32, # 38 p. 5179 - 5182
反应条件
Ni(PPh3)4 in tetrahydrofuran; diethyl ether 2 h; Ambient temperature;
参考文献
Clayden, Jonathan; Cooney, J. Jonathan A.; Julia, Marc
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 1 p. 7 - 14
反应条件
nickel in tetrahydrofuran T=20°C; Tamao-Kumada-Corriu reaction; 24 h;
参考文献
Phan, Nam T.S.; Brown, David H.; Adams, Harry; Spey, Sharon E.; Styring, Peter
Dalton Transactions, 2004 , # 9 p. 1348 - 1357
反应条件
1: diethyl ether / anschliessendes Kochen mit CuCl2 2: butyl lithium; diethyl ether; benzene / anschliessend mit festem Kohlendioxid behandeln 3: isoquinoline; copper-powder View Scheme
参考文献
Gilman; Swiss; Cheney
Journal of the American Chemical Society, 1940 , vol. 62, p. 1963,1965
反应条件
1: aqueous NaOH 2: butyl lithium; diethyl ether; benzene / anschliessend mit festem Kohlendioxid behandeln 3: isoquinoline; copper-powder View Scheme
参考文献
Gilman; Swiss; Cheney
Journal of the American Chemical Society, 1940 , vol. 62, p. 1963,1965
反应条件
1: butyl lithium; diethyl ether; benzene / anschliessend mit festem Kohlendioxid behandeln 2: isoquinoline; copper-powder View Scheme
参考文献
Gilman; Swiss; Cheney
Journal of the American Chemical Society, 1940 , vol. 62, p. 1963,1965
反应条件
1: With n-butyllithium; CuCl2*TMEDA in tetrahydrofuran; hexanes T=20°C; 2 h; Inert atmosphere; 2: With iodine in tetrahydrofuran; hexanes T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Nguyen, Tan Tai; Marquise, Nada; Chevallier, Floris; Mongin, Florence
Chemistry - A European Journal, 2011 , vol. 17, # 37 p. 10405 - 10416
反应条件
[2,2']bipyridinyl; potassium iodide; NiBr2bipy in various solvent(s) Ambient temperatureelectrochemical coupling; Yields of byproduct given;
参考文献
Meyer, Gilbert; Rollin, Yolande; Perichon, Jacques
Journal of Organometallic Chemistry, 1987 , vol. 333, p. 263 - 268
