反应条件
1.1: 80 percent / sodium / tetrahydrofuran / 13 h / 0 - 20 °C 2.1: 71 percent / aq. H2O2; trifluoroacetic anhydride; Na2CO3 / CH2Cl2 / 3 h / 20 °C 3.1: 96 percent / PPTS / acetone / 16 h / 20 °C 4.1: sodium / 24 h / 90 °C 4.2: 60 percent / aq. HCl / tetrahydrofuran / 20 °C 5.1: methanol / 10percent Pd/C / 6 h / Heating 5.2: aq. HCl / 80 °C 5.3: 85 percent / H2 / 10percent Pd/C / methanol; H2O / 12 h View Scheme
参考文献
Podeschwa, Michael; Plettenburg, Oliver; Vom Brocke, Jochen; Block, Oliver; Adelt, Stephan; Altenbach, Hans-Josef
European Journal of Organic Chemistry, 2003 , # 10 p. 1958 - 1972
