2,3,4,5-四甲基苯酚合成路线 （共 26 条）
反应条件
sulfuric acid; mercury(II) oxide
Heating;
参考文献
Plouin,D.; Glenat,R.
Bulletin de la Societe Chimique de France, 1975 , p. 336 - 338
反应条件
2: methanol
3: copper oxide-chromium oxide; dioxane / 180 °C / 154457 Torr / Hydrogenation
View Scheme
参考文献
Fitzgerald
Journal of Applied Chemistry, 1955 , vol. 5, p. 289,293
反应条件
1: N2H4+H2O; KOH; diethylene glycol
2: pyridine hydrochloride
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: methanol
2: copper oxide-chromium oxide; dioxane / 180 °C / 154457 Torr / Hydrogenation
View Scheme
参考文献
Fitzgerald
Journal of Applied Chemistry, 1955 , vol. 5, p. 289,293
反应条件
1: POCl3
2: N2H4+H2O; KOH; diethylene glycol
3: pyridine hydrochloride
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: POCl3
2: N2H4+H2O; KOH; diethylene glycol
3: POCl3
4: N2H4+H2O; KOH; diethylene glycol
5: pyridine hydrochloride
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: diethyl ether; AlCl3; HCl / anschliessenden Behandeln mit H2O
2: amalgamated zinc; aq.-ethanolic HCl
View Scheme
参考文献
Fitzgerald
Journal of Applied Chemistry, 1955 , vol. 5, p. 289,293
反应条件
1: N2H4+H2O; KOH; diethylene glycol
2: POCl3
3: N2H4+H2O; KOH; diethylene glycol
4: pyridine hydrochloride
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: copper oxide-chromium oxide; dioxane / 200 °C / Hydrogenation
2: methanol
3: copper oxide-chromium oxide; dioxane / 180 °C / 154457 Torr / Hydrogenation
View Scheme
参考文献
Fitzgerald
Journal of Applied Chemistry, 1955 , vol. 5, p. 289,293
反应条件
sodium hydroxide; perchloric acid
1.) H2O, 80 deg C, 35 - 40 min, 2.) H2O, water, reflux, 3 h; Multistep reaction;
参考文献
Rajoharison, H. G.; Soltani, H.; Arnaud, M.; Roussel, C.; Metzger, J.; Poincare, Rue H.
Synthetic Communications, 1980 , vol. 10, # 3 p. 195 - 204
