1-甲基-3-(甲硫基)苯合成路线 (共 23 条)
反应条件
sodium hydroxide; Aliquatreg; 336 1) H2O-C6H6, room temperature, 2 h, 2) room temperature, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Sugawara; Shirahata; Sato
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 11 p. 3353 - 3354
反应条件
tetrachloromethane; N-bromosuccinmide
参考文献
Chemische Berichte, , vol. 92, p. 2887,2891
反应条件
1: 1) n-butyllithium , 2) Raney-Ni View Scheme
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna; Melis, Stefana; Sotgiu, Francesca
Tetrahedron, 1990 , vol. 46, # 3 p. 861 - 884
反应条件
n-butyllithium; nickel Multistep reaction;
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna; Melis, Stefana; Sotgiu, Francesca
Tetrahedron, 1990 , vol. 46, # 3 p. 861 - 884
反应条件
1: 1) n-butyllithium , 2) Raney-Ni View Scheme
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna; Melis, Stefana; Sotgiu, Francesca
Tetrahedron, 1990 , vol. 46, # 3 p. 861 - 884
反应条件
1: aqueous H2O2; acetic acid 2: KMnO4 View Scheme
参考文献
Kloosterziel; Backer
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 295,299
Recueil des Travaux Chimiques des Pays-Bas, 1953 , vol. 72, p. 185,194
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; sodium hydride; diethylamine in xylene 6 h; Heating;
参考文献
Cabiddu, S.; Melis, S.; Piras, P. P.; Sotgiu, F.
Synthesis, 1982 , # 7 p. 583 - 584
反应条件
aluminium trichloride; phosphorus trichoride 2 h; Heating; Yields of byproduct given;
参考文献
Baccolini, Graziano; Mezzina, Elisabetta; Todesko, Paolo Edgardo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3281 - 3284
反应条件
n-butyllithium; potassium tert-butylate 1) hexane, -60 to -10 deg C, 2) hexane, RT, overnight; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Melis, Stefana; Serci, Alessandro
Tetrahedron, 1994 , vol. 50, # 20 p. 6037 - 6048
反应条件
n-butyllithium; nickel Multistep reaction;
参考文献
Cabiddu, Salvatore; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna; Melis, Stefana; Sotgiu, Francesca
Tetrahedron, 1990 , vol. 46, # 3 p. 861 - 884