6-甲基-2-(4-硝基苯基)苯并噻唑合成路线 （共 5 条）
反应条件
palladium 10 on activated carbon; hydrogen in dichloromethane T=25°C; 4 h; Inert atmosphere;
参考文献
Hu, Wan-Ping; Chen, Yin-Kai; Liao, Chao-Cheng; Yu, Hsin-Su; Tsai, Yi-Min; Huang, Shu-Mei; Tsai, Feng-Yuan; Shen, Ho-Chuan; Chang, Long-Sen; Wang, Jeh-Jeng
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 16 p. 6197 - 6207
反应条件
1: With potassium carbonate in water; N,N-dimethyl-formamide
Suzuki-Miyaura Coupling; 1 h; Inert atmosphere;
2: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water; N,N-dimethyl-formamide
T=80°C; Suzuki-Miyaura Coupling; 5 h; Inert atmosphere;
参考文献
Bort, Guillaume; Sylla-Iyarreta Veitia, Maite; Ferroud, Clotilde
Tetrahedron, 2013 , vol. 69, # 35 p. 7345 - 7353
反应条件
in neat (no solvent)
0.5 h; Green chemistry; Time;
参考文献
Yoon, Soon Byung; Chun, Eun Jeong; Noh, Young Ri; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 9 p. 2819 - 2821
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in ethanol; water
T=90°C;
参考文献
Hu, Wan-Ping; Chen, Yin-Kai; Liao, Chao-Cheng; Yu, Hsin-Su; Tsai, Yi-Min; Huang, Shu-Mei; Tsai, Feng-Yuan; Shen, Ho-Chuan; Chang, Long-Sen; Wang, Jeh-Jeng
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 16 p. 6197 - 6207
反应条件
hydrogenchloride; potassium dichromate; sulfuric acid
参考文献
Fridman
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1807,1811; engl. Ausg. S. 1871, 1874, 1875
