3,4-二氢-4-苯基-2(1H)-喹啉合成路线 (共 30 条)
反应条件
HUSY in 1,2-dichloro-benzene
T=190°C; 27 h;
参考文献
Koltunov, Konstantin Yu.; Walspurger, Stephane; Sommer, Jean
Chemical Communications, 2004 , # 15 p. 1754 - 1755
反应条件
hydrogen; 1,4-di(diphenylphosphino)-butane; 1-n-butyl-3-methylimidazolium hexafluorophosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex
T=120°C; P=31028.9 Torr; 45 h;
参考文献
Ye, Fangguo; Alper, Howard
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 14 p. 1855 - 1861
反应条件
1: With trifluoroacetic acid
T=110°C;
2: With sodium hydrogencarbonate in water
参考文献
Park, Ja Ock; Youn, So Won
Organic Letters, 2010 , vol. 12, # 10 p. 2258 - 2261
反应条件
triethylaluminum; pyridine; bis(acetylacetonate)nickel(II) in pyridine; toluene
T=80 - 100°C; 5 h;
参考文献
Canoira, Laureano; Rodriguez, J. Gonzalo
Journal of Chemical Research, Miniprint, 1988 , # 2 p. 646 - 666
反应条件
hydrogenchloride; zinc in ethanol; water
RefluxInert atmosphere;
参考文献
Shang, Rui; Huang, Zheng; Chu, Ling; Fu, Yao; Liu, Lei
Organic Letters, 2011 , vol. 13, # 16 p. 4240 - 4243
反应条件
ziconium(IV) oxychloride octahydrate in neat (no solvent)
T=30 - 40°C; 0.75 h; Sonication;
参考文献
Azarifar, Davood; Sheikh, Davood
Synthetic Communications, 2013 , vol. 43, # 18 p. 2517 - 2526
反应条件
trifluorormethanesulfonic acid
T=20°C; 5 h;
参考文献
Koltunov, Konstantin Yu.; Prakash, G. K. Surya; Rasul, Golam; Olah, George A.
Heterocycles, 2004 , vol. 62, p. 757 - 772
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; potassium hydroxide in 1,4-dioxane; water
Michael condensation; 2 h; RefluxInert atmosphere;
参考文献
Horn, Joachim; Li, Ho Yin; Marsden, Stephen P.; Nelson, Adam; Shearer, Rachel J.; Campbell, Amanda J.; House, David; Weingarten, Gordon G.
Tetrahedron, 2009 , vol. 65, # 44 p. 9002 - 9007
反应条件
pyridine; bis(acetylacetonate)nickel(II) in pyridine; toluene
T=80 - 100°C; 5 h;
参考文献
Canoira, Laureano; Rodriguez, J. Gonzalo
Journal of Chemical Research, Miniprint, 1988 , # 2 p. 646 - 666
反应条件
phosphorous pentoxide
T=80 - 110°C;
参考文献
Kaboudin, Babak; Abedi, Yaghoub
Organic Preparations and Procedures International, 2009 , vol. 41, # 3 p. 229 - 236