反应条件
1: diisobutylaluminum hydride / tetrahydrofuran; hexane / -78 °C 2: pyridinium chlorochromate / CH2Cl2 / 1.5 h / Ambient temperature 3: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, RT 4: manganese dioxide / benzene / 3 h / Ambient temperature View Scheme
参考文献
Wadsworth, Donald H.; Geer, Susan M.; Detty, Michael R.
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3662 - 3668