2,3,4,5-四氯苯酚合成路线 (共 23 条)
反应条件
(i) Cu2O, H2SO4, EtOH, (ii) Cu; Multistep reaction;
参考文献
Huisgen,R. et al.
Chemische Berichte, 1964 , vol. 97, p. 2868 - 2883
反应条件
(i) NaNO2, H2SO4, (ii) aq. CuSO4; Multistep reaction;
参考文献
Howe,R.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 478 - 480
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide 24 h; Ambient temperatureother reaction times; Product distributionMechanism;
参考文献
Mach, Martin H.; Bunnett, Joseph F.
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4660 - 4666
反应条件
water T=25°C; Rate constant;
参考文献
Chrystiuk, Edwin; Jusoh, Adelina; Santafianos, Dino; Williams, Andrew
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 163 - 168
反应条件
Irradiation; Yield given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Lelgemann, Rudolf
Chemische Berichte, 1991 , vol. 124, # 8 p. 1865 - 1866
反应条件
T=176 - 180°C; im Rohr; Kinetics;
参考文献
Holleman
Recueil des Travaux Chimiques des Pays-Bas, 1920 , vol. 39, p. 748
Recueil des Travaux Chimiques des Pays-Bas, 1921 , vol. 40, p. 318
反应条件
T=20°C; Irradiationother o-chinone diazide; var. MeOH/ oxetane ratios; Product distribution;
参考文献
Kirmse, Wolfgang; Lelgemann, Rudolf
Chemische Berichte, 1991 , vol. 124, # 8 p. 1865 - 1866
反应条件
T=990°C; 0.00555556 h; other polychlorophenols and their sodium salts, other temp. and times; Product distributionMechanism;
参考文献
Bassoli, Angela; Parrilli, Daniele; Rindone, Bruno; Pitea, Demetrio; Siniscalco, Falco
Gazzetta Chimica Italiana, 1990 , vol. 120, # 5 p. 333 - 339
反应条件
aluminium trichloride; chlorine; iron T=120 - 195°C;
参考文献
Dow Chem. Co.
Patent: US2131259 , 1937 ;
反应条件
in water; acetonitrile 6 h; Irradiationvarying reaction time, pH of photolyzed sample; Product distributionMechanism;
参考文献
Choudhry, Ghulam Ghaus; Wielen, Frans W. M. van der; Webster, G. R. Barrie; Hutzinger, Otto
Canadian Journal of Chemistry, 1985 , vol. 63, p. 469 - 475