3-甲基-6-(1-甲基乙亚基)环己-2-烯-1-酮合成路线 （共 58 条）
反应条件
sodium hydroxide; Mucor piriformis in acetone T=29 - 30°C; 48 h; Further byproducts given;
参考文献
Madyastha; Thulasiram
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 3 p. 1203 - 1207
反应条件
sodium hydroxide; Mucor piriformis in acetone T=29 - 30°C; 48 h; Further byproducts given;
参考文献
Madyastha; Thulasiram
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 3 p. 1203 - 1207
反应条件
1: 30 percent Chromat. / H2O / 264 h / Mucor plumbeus 2: 0.1 N HCl / 25 °C View Scheme
参考文献
Ismaili-Alaoui; Benjilali; Buisson; Azerad
Tetrahedron Letters, 1992 , vol. 33, # 17 p. 2349 - 2352
反应条件
1,2-benzenedicarboxylic acid in water Title compound not separated from byproducts;
参考文献
Boggiatto, Margarita V. de; Heluani, Carola S. de; Fenik, Ines J. S.; Catalan, Cesar A. N.
Journal of Organic Chemistry, 1987 , vol. 52, # 8 p. 1505 - 1511
反应条件
hydrogenchloride T=25°C;
参考文献
Ismaili-Alaoui; Benjilali; Buisson; Azerad
Tetrahedron Letters, 1992 , vol. 33, # 17 p. 2349 - 2352
反应条件
sodium acetate; acetic anhydride; acetic acid 12 h; Heating;
参考文献
Kulkarni, Yashwant S.; Niwa, Maho; Ron, Eyal; Snider, Barry B.
Journal of Organic Chemistry, 1987 , vol. 52, # 8 p. 1568 - 1576
反应条件
air T=120°C; Oxidation; Thermolysis;
参考文献
Mcgraw, Gerald W.; Hemingway, Richard W.; Ingram Jr., Leonard L.; Canady, Catherine S.; Mcgraw, William B.
Environmental Science and Technology, 1999 , vol. 33, # 22 p. 4029 - 4033
反应条件
trifluorormethanesulfonic acid 40 h; Ambient temperatureIrradiation; Further byproducts given;
参考文献
Baeckstroem, Peter; Jacobsson, Ulla; Koutek, Bohumir; Norin, Torbjoern
Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3728 - 3732
反应条件
1.1: N,N,N',N'-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C 1.2: N,N,N',N'-tetramethylethylenediamine; O2 / hexane; tetrahydrofuran / 7 h / 20 °C 2.1: 83 percent / sodium borohydride / 2-methyl-propan-2-ol / 1 h / Heating 3.1: 72 percent / oxalyl chloride; DMSO; triethylamine / CH2Cl2 / -60 - 20 °C View Scheme
参考文献
Baptistella, Lucia H. B.; Aleixo, Adriana M.
Synthetic Communications, 2002 , vol. 32, # 19 p. 2937 - 2950
反应条件
1: 83 percent / sodium borohydride / 2-methyl-propan-2-ol / 1 h / Heating 2: 72 percent / oxalyl chloride; DMSO; triethylamine / CH2Cl2 / -60 - 20 °C View Scheme
参考文献
Baptistella, Lucia H. B.; Aleixo, Adriana M.
Synthetic Communications, 2002 , vol. 32, # 19 p. 2937 - 2950
