1-甲基-1,2,3,4-四氢喹啉合成路线 (共 86 条)
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) THF, hexane, 0 deg C, 2.) 12 h, rt;
参考文献
Ahlbrecht,H.; Duebner,E.O.
Tetrahedron, 1984 , vol. 40, p. 1157
反应条件
sodium hydrogencarbonate in water; ethyl acetate 2.5 h; Ambient temperature;
参考文献
THE WELLCOME FOUNDATION LIMITED
Patent: EP96214 B1, 1991 ;
反应条件
Decaborane in methanol; water T=20°C; 0.5 h;
参考文献
Yeon Joo Jung; Jong Woo Bae; Choon-Ock Maing Yoon; Byung Woo Yoo; Cheol Min Yoon
Synthetic Communications, 2001 , vol. 31, # 22 p. 3417 - 3421
反应条件
LiH3BNMe2 in tetrahydrofuran T=65°C; 2 h;
参考文献
Flaniken, John M.; Collins, Christopher J.; Lanz, Marc; Singaram, Bakthan
Organic Letters, 1999 , vol. 1, # 5 p. 799 - 801
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=20°C; 24 h;
参考文献
Hu, Wan-Ping; Tsai, Pei-Ching; Hsu, Ming-Kuan; Wang, Jeh-Jeng
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3983 - 3985
反应条件
borane-THF in tetrahydrofuran T=20°C; 24 h;
参考文献
Hu, Wan-Ping; Tsai, Pei-Ching; Hsu, Ming-Kuan; Wang, Jeh-Jeng
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3983 - 3985
反应条件
borane-THF in tetrahydrofuran T=20°C; 24 h;
参考文献
Hu, Wan-Ping; Tsai, Pei-Ching; Hsu, Ming-Kuan; Wang, Jeh-Jeng
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3983 - 3985
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=20°C; 24 h;
参考文献
Hu, Wan-Ping; Tsai, Pei-Ching; Hsu, Ming-Kuan; Wang, Jeh-Jeng
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3983 - 3985
反应条件
disodium hydrogenphosphate; sodium amalgam in methanol T=25°C;
参考文献
Padwa, Albert; Gareau, Yves; Harrison, Brian; Rodriguez, Augusto
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3540 - 3545
反应条件
lithium aluminium tetrahydride
参考文献
Gawinecki, Ryszard; Kolehmainen, Erkki; Kauppinen, Reijo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1998 , # 1 p. 25 - 30