2,4-二羟基-6-戊基苯甲酸合成路线 （共 15 条）
反应条件
palladium 10 on activated carbon; hydrogen in ethyl acetate
T=20°C; P=750.075 Torr; 24 h;
参考文献
Lin, Hao; Annamalai, Thirunavukkarasu; Bansod, Priyanka; Tse-Dinh, Yuk-Ching; Sun, Dianqing
MedChemComm, 2013 , vol. 4, # 12 p. 1613 - 1618
反应条件
sodium chlorite; sodium dihydrogenphosphate in water; dimethyl sulfoxide
T=0 - 20°C; 14 h;
参考文献
Lin, Hao; Annamalai, Thirunavukkarasu; Bansod, Priyanka; Tse-Dinh, Yuk-Ching; Sun, Dianqing
MedChemComm, 2013 , vol. 4, # 12 p. 1613 - 1618
反应条件
sodium acetate in ethanol
参考文献
Harris,T.M.; Carney,R.L.
Journal of the American Chemical Society, 1967 , vol. 89, p. 6734 - 6741
反应条件
hydrogen; sodium hydrogencarbonate; palladium on activated charcoal
Ambient temperature;
参考文献
Shibuya; Ebizuka; Noguchi; Iitaka; Sankawa
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 407 - 413
反应条件
1: 48 percent / conc. H2SO4 / 1 h / Ambient temperature
2: 71 percent / NaHCO3, H2 / Pd-C (10percent) / Ambient temperature
View Scheme
参考文献
Shibuya; Ebizuka; Noguchi; Iitaka; Sankawa
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 407 - 413
反应条件
1: trichlorophosphate / 18 h / 0 - 20 °C
2: sodium dihydrogenphosphate; sodium chlorite / dimethyl sulfoxide; water / 14 h / 0 - 20 °C
View Scheme
参考文献
Lin, Hao; Annamalai, Thirunavukkarasu; Bansod, Priyanka; Tse-Dinh, Yuk-Ching; Sun, Dianqing
MedChemComm, 2013 , vol. 4, # 12 p. 1613 - 1618
反应条件
sulfuric acid
anschliessend Behandeln mit Wasser;
参考文献
Fujii; Osumi
Yakugaku Zasshi, 1937 , vol. 57, p. 134,139
Chem.Abstr., 1939 , p. 3371
参考文献
Asahina; Fujikawa
Chemische Berichte, 1935 , vol. 68, p. 634,636, 638
反应条件
sulfuric acid
anschliessend Behandeln mit Wasser;
参考文献
Fujii; Osumi
Yakugaku Zasshi, 1937 , vol. 57, p. 134,139
Chem.Abstr., 1939 , p. 3371
参考文献
Asahina; Nogami
Chemische Berichte, 1937 , vol. 70, p. 1498
