2,3-二氢-1,1-二甲基-1H-茚合成路线 (共 48 条)
反应条件
hydrogenchloride; AlCl3, aluminium chloride; (+)-(1R,5R)-α-pinene in hexane
T=20°C; Friedel Crafts alkylation;
参考文献
Wang, Jie; Zhou, Pengfei; Wang, Yang
European Journal of Organic Chemistry, 2011 , # 2 p. 264 - 270
反应条件
epoxysulfonyl fluoride in dichloromethane
T=-78°C; 0.5 h;
参考文献
Barrow, Colin J.; Bright, Steven T.; Coxon, James M.; Steel, Peter J.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2542 - 2549
反应条件
1: diethyl ether
2: aq. H2SO4
View Scheme
参考文献
Warrick,P.; Saunders,W.H.
Journal of the American Chemical Society, 1962 , vol. 84, p. 4095 - 4100
反应条件
copper oxide-chromium oxide
Hydrogenation.anschliessend an Palladium/Kohle hydrieren;
参考文献
Schaap; Pines
Journal of the American Chemical Society, 1957 , vol. 79, p. 4967,4968
反应条件
triethyl borane; tri-n-butyl-tin hydride in hexane; benzene
T=20°C; 1 h;
参考文献
Miura, Katsukiyo; Ichinose, Yoshifumi; Nozaki, Kyoko; Fugami, Keigo; Oshima, Koichiro; Utimoto, Kiitiro
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 1 p. 143 - 147
反应条件
T=-196.1°C; P=5E-05 Torr;
参考文献
Armstrong, Brian M.
Journal of the American Chemical Society, 1998 , vol. 120, # 24 p. 6007 - 6011
反应条件
1: Mg / Grignard reaction
2: 85percent H2SO4
View Scheme
参考文献
Sakhabutdinov, A. G.; Usmanova, A. G.; Frolov, P. A.; Kushnarev, D. F.; Schmidt, F. K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1452 - 1455
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1610 - 1614
参考文献
Sekiguchi, Akira; Ando, Wataru
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5286 - 5290
反应条件
T=500°C; P=3 Torr; Pyrolyse;
参考文献
Sekiguchi, Akira; Ando, Wataru
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5286 - 5290
反应条件
in dichloromethane
2 h; -40 to 0 deg C;
参考文献
Reetz, Manfred T.; Westermann, Juergen; Steinbach, Rainer
Journal of the Chemical Society, Chemical Communications, 1981 , # 5 p. 237 - 239