5-(二甲氨基)间二甲苯合成路线 （共 23 条）
反应条件
triethylamine in acetonitrile T=-40°C; 6 h;
参考文献
Vernaudon, Pascal; Rajoharison, Harivelo G.; Roussel, Chritian
Bulletin de la Societe Chimique de France, 1987 , # 1 p. 205 - 211
反应条件
1: With N,N-dimethylthiocarbamoyl chloride in dichloromethane T=20°C; 2 h; 2: in acetonitrile 3 h; Reflux;
参考文献
Caliskan, Hafize; Zaim, Oemer
Synthetic Communications, 2010 , vol. 40, # 20 p. 3078 - 3083
反应条件
sodium hydride in tetrahydrofuran T=20°C; 3 h;
参考文献
Saitoh, Terunobu; Yoshida, Suguru; Ichikawa, Junji
Journal of Organic Chemistry, 2006 , vol. 71, # 17 p. 6414 - 6419
反应条件
sodium tetrahydroborate; sulfuric acid in tetrahydrofuran T=10 - 30°C; Yield given;
参考文献
Giuamanini, Angelo G.; Chiavari, Giuseppe; Musiani, Marco M.; Rossi, Patrizia
Synthesis, 1980 , # 9 p. 743 - 746
参考文献
Dimroth,K.
Angewandte Chemie, 1960 , vol. 72, p. 331 - 342
反应条件
1: natrium carbonate; water 2: durch Ueberfuehren in die quartaere Base und Destillieren View Scheme
参考文献
Noelting; Trautmann
Chemische Berichte, 1891 , vol. 24, p. 563 Anm.
反应条件
durch Reduktion und anschliessende Methylierung;
参考文献
Crocker; Jones
Journal of the Chemical Society, 1959 , p. 1808,1809
反应条件
durch Ueberfuehren in die quartaere Base und Destillieren;
参考文献
Noelting; Trautmann
Chemische Berichte, 1891 , vol. 24, p. 563 Anm.
反应条件
T=51.9°C; ΔG0; Equilibrium constantThermodynamic data;
参考文献
Lias, Sharon G.; Jackson, Jo-Anne A.; Argentar, Harold; Liebman, Joel F.
Journal of Organic Chemistry, 1985 , vol. 50, # 3 p. 333 - 338
反应条件
T=51.9°C; ΔG0; Equilibrium constantThermodynamic data;
参考文献
Lias, Sharon G.; Jackson, Jo-Anne A.; Argentar, Harold; Liebman, Joel F.
Journal of Organic Chemistry, 1985 , vol. 50, # 3 p. 333 - 338
