反应条件
1: thien-2-yl bromide With magnesium in diethyl ether T=20°C; 0.5 h; 2: 2,5-dibromo-3-(5,5-dimethyl-1,3-dioxan-2-yl)thiophene With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in diethyl ether Kumada coupling; 4 h; Heating;
参考文献
Collis, Gavin E.; Burrell, Anthony K.; Scott, Sonya M.; Officer, David L.
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 8974 - 8983