1-苯酰基-3-苯基硫脲合成路线 （共 36 条）
反应条件
in acetone T=20°C; 1 h;
参考文献
Wang, Xuemei; Xu, Feng; Xu, Qingge; Mahmud, Hossen; Houze, Jonathan; Zhu, Liusheng; Akerman, Michelle; Tonn, George; Tang, Liang; McMaster, Brian E.; Dairaghi, Daniel J.; Schall, Thomas J.; Collins, Tassie L.; Medina, Julio C.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 10 p. 2800 - 2803
反应条件
1: ammonium thiocyanate; benzoyl chloride With PEG-400 in dichloromethane T=20°C; Substitution; 1 h; 2: aniline in dichloromethane T=20°C; Addition; 1 h;
参考文献
Wei, Tai-Bao; Zhang, You-Ming; Gao, Li-Ming
Synthetic Communications, 2000 , vol. 30, # 3 p. 493 - 500
反应条件
sodium acetate in methanol T=50°C; 0.0833333 h;
参考文献
Kavalek, Jaromir; Jirman, Josef; Sterba, Vojeslav
Collection of Czechoslovak Chemical Communications, 1985 , vol. 50, # 3 p. 766 - 778
反应条件
1: sodium isothiocyanate; benzoyl chloride in acetone T=0°C; Substitution; 2: aniline in acetone T=20°C; Addition;
参考文献
Chan, Chung Woo; Ng, Chun Ming Dominic; Ho, Joyce; Tin, Kam Chung
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 3 p. 216 - 219
反应条件
1: SiO2 / 1,2-dichloro-ethane / 2 h / 25 °C 2: 1,2-dichloro-ethane / 1 h / 25 °C View Scheme
参考文献
Rasmussen, C. R.; Villani, F. J.; Weaner, L. E.; Reynolds, B. E.; Hood, A. R.; et al.
Synthesis, 1988 , # 6 p. 456 - 459
参考文献
Wheeler; Sanders
Journal of the American Chemical Society, 1900 , vol. 22, p. 377
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Wheeler
Journal of the American Chemical Society, 1901 , vol. 23, p. 225
反应条件
in acetone 3 h; Heating;
参考文献
Kavalek, Jaromir; Jirman, Josef; Machacek, Vladimir; Sterba, Vojeslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 3 p. 593 - 600
反应条件
1: 56 percent / acetone / 4 h / Heating 2: 84 percent / conc. HCl, 30percent H2O2 / ethanol / 0.08 h / Heating 3: 80 percent / 25percent aq. NH4OH / ethanol / 20 °C 4: 48 percent / ethanol / 1 h / Heating View Scheme
参考文献
Wheeler; Sanders
Journal of the American Chemical Society, 1900 , vol. 22, p. 377
反应条件
1: 84 percent / conc. HCl, 30percent H2O2 / ethanol / 0.08 h / Heating 2: 80 percent / 25percent aq. NH4OH / ethanol / 20 °C 3: 48 percent / ethanol / 1 h / Heating View Scheme
参考文献
Saczewski, Franciszek; Foks, Henryk
Synthesis, 1986 , # 9 p. 751 - 753
反应条件
1: 80 percent / 25percent aq. NH4OH / ethanol / 20 °C 2: 48 percent / ethanol / 1 h / Heating View Scheme
参考文献
Saczewski, Franciszek; Foks, Henryk
Synthesis, 1986 , # 9 p. 751 - 753
