5-苄基-4-苯基咪唑烷-2,4-二酮合成路线 （共 6 条）
反应条件
1: benzonitrile; chloro(phenylmethyl)-magnesium With copper(l) iodide in tetrahydrofuran
T=70°C; 24 h;
2: (NH4)2CO3 With potassium cyanide in tetrahydrofuran; ethanol; water
T=75°C; 24 h;
参考文献
Montagne, Cyril; Shipman, Michael
Synlett, 2006 , # 14 p. 2203 - 2206
反应条件
1: With potassium hydroxide in ethanol
T=50°C; 0.75 h; Sonication;
2: With hydrogenchloride in ethanol; water
pH=5 - 6;
参考文献
Li, Ji-Tai; Xu, Xiao-Ya; Yin, Ying
Letters in Organic Chemistry, 2011 , vol. 8, # 3 p. 198 - 201
反应条件
in ethanol; water
Heating;
参考文献
Trisovic, Nemanja; Valentic, Natasa; Erovic, Marko; Dakovic-Sekulic, Tatjana; Uscumlic, Gordana; Juranic, Ivan
Monatshefte fur Chemie, 2011 , vol. 142, # 12 p. 1227 - 1234
反应条件
ethanol
P=14710.2 Torr; Erwaermen unter CO2;
参考文献
Slotta; Behnisch; Szyszka
Chemische Berichte, 1934 , vol. 67, p. 1529,1533
反应条件
potassium hydroxide; ethanol
参考文献
Enebaeck
Acta Chemica Scandinavica (1947-1973), 1958 , vol. 12, p. 1528
反应条件
barium dihydroxide in water
T=160 - 180°C;
参考文献
Goodson,L.H. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1920 - 1924
