3,4-二氢-1H-苯并吡喃合成路线 （共 99 条）
反应条件
T=413°C; P=170 Torr; 4.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Paul, Gitendra C.; Gajewski, Joseph J.
Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5060 - 5062
反应条件
T=413°C; P=1 - 1.5 Torr; 4.5 h; other pressure; also in the presence of H2 or cis- and trans-2-butene; Product distributionMechanism;
参考文献
Paul, Gitendra C.; Gajewski, Joseph J.
Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5060 - 5062
反应条件
in toluene T=609.9°C; MechanismKinetics;
参考文献
Journal of Organic Chemistry, , vol. 62, # 14 p. 4804 - 4810
反应条件
acetic acid; zinc
T=100°C;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GmbH; CARSON, Rebekah J.; FADER, Lee; KAWAI, Stephen; LANDRY, Serge
Patent: WO2009/62288 A1, 2009 ;
Location in patent: Page/Page column 72-73 ;
反应条件
1: With acetic anhydride in acetic acid
3 h; Heating / reflux;
2: With hydrogen; palladium 10 on activated carbon
P=2172.08 Torr;
参考文献
VERNALIS RESEARCH LIMITED
Patent: US2005/187282 A1, 2005 ;
Location in patent: Page/Page column 10 ;
US 20050187282 A1
反应条件
H2; palladium monocarbide in acetic acid; ethyl acetate
参考文献
Eli Lilly and Company
Patent: US5352690 A1, 1994 ;
US 5352690 A
反应条件
copper(l) iodide; 8-hydroxy-quinoline; caesium carbonate in toluene
T=20 - 110°C; Inert atmosphere;
参考文献
Niu, Jiajia; Guo, Pengran; Kang, Juntao; Li, Zhigang; Xu, Jingwei; Hu, Shaojing
Journal of Organic Chemistry, 2009 , vol. 74, # 14 p. 5075 - 5078
反应条件
2-(di-t-butylphosphino)-1,1'-binaphthyl; palladium diacetate; caesium carbonate in toluene
T=65°C; 21 h;
参考文献
Toracca, Karen E.; Kuwabe, Shin-Itsu; Buchwald, Stephen L.
Journal of the American Chemical Society, 2000 , vol. 122, # 51 p. 12907 - 12908
反应条件
hydrogen; 10percent Pd/C in chloroform
T=20°C; 12 h; ambient pressure;
参考文献
Boyd, Derek R.; Sharma, Narain D.; Bowers, Nigel I.; Boyle, Rosemary; Harrison, John S.; Lee, Kyoung; Bugg, Timothy D.H.; Gibson, David T.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 8 p. 1298 - 1307
反应条件
gold(III) chloride; silver trifluoromethanesulfonate in 1,2-dichloro-ethane
T=120°C; 48 h;
参考文献
Shi, Zhangjie; He, Chuan
Journal of the American Chemical Society, 2004 , vol. 126, # 42 p. 13596 - 13597
