3,4-二氢-1H-苯并吡喃合成路线 （共 99 条）
反应条件
indium tribromide in chloroform
参考文献
Lagoutte, Roman; Wilkinson, James A.
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6942 - 6944
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / |Inert atmosphere
1.2: 20 h / -78 - 20 °C / |Inert atmosphere
2.1: [Rh2(trifluoroacetate)4] / toluene / 4 h / 80 °C / |Inert atmosphere
3.1: palladium on activated charcoal; hydrogen / methanol / 12 h / 20 °C / 760.05 Torr
View Scheme
参考文献
Murase, Hirohiko; Senda, Kousuke; Senoo, Masato; Hata, Takeshi; Urabe, Hirokazu
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 317 - 322
反应条件
1: [Rh2(trifluoroacetate)4] / toluene / 4 h / 80 °C / |Inert atmosphere
2: palladium on activated charcoal; hydrogen / methanol / 12 h / 20 °C / 760.05 Torr
View Scheme
参考文献
Murase, Hirohiko; Senda, Kousuke; Senoo, Masato; Hata, Takeshi; Urabe, Hirokazu
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 317 - 322
反应条件
1.1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere
1.2: |Inert atmosphere
2.1: triethylamine / dichloromethane / 0 - 20 °C / |Inert atmosphere
3.1: cesium hydroxide monohydrate / N,N-dimethyl-formamide / 0 °C / |Inert atmosphere
3.2: 0 - 20 °C / |Inert atmosphere
4.1: phenyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Willand-Charnley, Rachel; Puffer, Benjamin W.; Dussault, Patrick H.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5821 - 5823
反应条件
1.1: cesium hydroxide monohydrate / N,N-dimethyl-formamide / 0 °C / |Inert atmosphere
1.2: 0 - 20 °C / |Inert atmosphere
2.1: phenyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Willand-Charnley, Rachel; Puffer, Benjamin W.; Dussault, Patrick H.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5821 - 5823
反应条件
1.1: cesium hydroxide monohydrate / N,N-dimethyl-formamide / 0 °C / |Inert atmosphere
1.2: 0 - 20 °C / |Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Willand-Charnley, Rachel; Puffer, Benjamin W.; Dussault, Patrick H.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5821 - 5823
反应条件
acetate buffer
T=40°C; other buffers; Rate constant;
参考文献
Knipe, Jay O.; Vasquez, Peter J.; Coward, James K.
Journal of the American Chemical Society, 1982 , vol. 104, # 11 p. 3202 - 3209
反应条件
indium tribromide in chloroform
参考文献
Lagoutte, Roman; Wilkinson, James A.
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6942 - 6944
反应条件
ethanol; Raney nickel (W4)
1 h; Heating;
参考文献
Sato, Kikumasa; Inoue, Seiichi; Miyamoto, Osamu; Ikeda, Hiroshi; Ota, Tomomi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4184 - 4186
参考文献
v. Braun; Steindorff
Chemische Berichte, 1905 , vol. 38, p. 855
