5-苯基-1,3-环己二酮合成路线 (共 57 条)
反应条件
1: With sulfuric acid
0.183333 h;
2: With iodine
T=85°C; 0.75 h; Reflux;
参考文献
Lebeuf, Raphael; Berlande, Muriel; Robert, Frederic; Landais, Yannick; Schrems, Marcus G.; Pfaltz, Andreas
Organic Syntheses, 2009 , vol. 86, p. 1 - 10
反应条件
1: Pd-C / diphenyl ether / Heating
View Scheme
参考文献
Nilsson,M.; Norin,T.
Acta Chemica Scandinavica (1947-1973), 1963 , vol. 17, # 4 p. 1157 - 1159
反应条件
potassium carbonate in acetone
16 h; Inert atmosphereReflux;
参考文献
Eddy, Nicholas A.; Kelly, Christopher B.; Mercadante, Michael A.; Leadbeater, Nicholas E.; Fenteany, Gabriel
Organic Letters, 2012 , vol. 14, # 2 p. 498 - 501
反应条件
1: aq. KOH / methanol
2: KOMe / methanol
View Scheme
参考文献
Stetter,H.; Sandhagen,H.-J.
Justus Liebigs Annalen der Chemie, 1968 , vol. 712, p. 67 - 72
参考文献
Desai
Journal of the Chemical Society, 1932 , p. 1079,1086
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Voitila <Fjaeder>
Annales Academiae Scientiarum Fennicae, Series A, 1937 , vol. 49, # 1 p. 18,68
反应条件
oxalyl dichloride in chloroform
1) slowly heated to boiling, 2 h, 2) reflux, 1.5 h;
参考文献
Piskov, V. B.; Kasperovich, V. P.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 6 p. 1088 - 1095
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 6 p. 1195 - 1203
参考文献
Boyd; Clifford; Probert
Journal of the Chemical Society, 1920 , vol. 117, p. 1388