2,4,6-三苯基三嗪合成路线 (共 216 条)
反应条件
ammonia; lanthanum trifluoromethanesulphonate T=200°C; 24 h; in a stainless steel pressure vessel;
参考文献
Forsberg, John H.; Spaziano, Vincent T.; Klump, Stephen P.; Sanders, Kathleen M.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 767 - 770
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene 48 h; Heating;
参考文献
Isfahani, Amir Landarani; Mohammadpoor-Baltork, Iraj; Mirkhani, Valiollah; Khosropour, Ahmad R.; Moghadam, Majid; Tangestaninejad, Shahram; Kia, Reza
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 957 - 972
反应条件
caesium carbonate in dimethyl sulfoxide T=90°C; 6 h;
参考文献
Biswas, Subhasish; Batra, Sanjay
European Journal of Organic Chemistry, 2012 , # 18 p. 3492 - 3499
反应条件
caesium carbonate in dimethyl sulfoxide T=90°C; 12 h; Inert atmosphere;
参考文献
Biswas, Subhasish; Batra, Sanjay
European Journal of Organic Chemistry, 2012 , # 18 p. 3492 - 3499
反应条件
{RuCl2(1-methyl-4-(1-methylethyl)benzene)}2; caesium carbonate in dimethyl sulfoxide T=110°C; 16 h; Sealed tube; Reagent/catalystSolventTimeTemperature;
参考文献
Xie, Feng; Chen, Mengmeng; Wang, Xiaoting; Jiang, Huanfeng; Zhang, Min
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 17 p. 2761 - 2768
反应条件
1: benzonitrile With AlCl3, aluminium chloride T=20 - 100°C; 2: 4-methoxy-aniline T=100°C; 4 h; 3: With sodium hydroxide in water T=20°C;
参考文献
Koutentis, Panayiotis A.; Mirallai, Styliana I.
Tetrahedron, 2010 , vol. 66, # 27-28 p. 5134 - 5139
反应条件
1: benzonitrile With AlCl3, aluminium chloride T=20 - 100°C; 2: aniline T=100°C; 4 h; 3: With sodium hydroxide in water T=20°C;
参考文献
Koutentis, Panayiotis A.; Mirallai, Styliana I.
Tetrahedron, 2010 , vol. 66, # 27-28 p. 5134 - 5139
反应条件
phosphorous pentoxide in diethyl ether T=0°C; P=1 Torr; 3 h; Inert atmosphere;
参考文献
Klenov, M. S.; Churakov, A. M.; Strelenko, Yu. A.; Tartakovsky, V. A.
Russian Chemical Bulletin, 2011 , vol. 60, # 11 p. 2429 - 2431,3
反应条件
SCl2 in benzene T=80°C; 2 h;
参考文献
Borovikova, G. S.; Levchenko, E. S.; Borovik, E. I.; Darmokhval, E. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 171 - 176
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 190 - 196
反应条件
trifluoromethylsulfonic anhydride in 1,2-dichloro-benzene T=20 - 120°C;
参考文献
Herrera, Antonio; Martinez-Alvarez, Roberto; Chioua, Rachid; Chioua, Mourad
Tetrahedron Letters, 2003 , vol. 44, # 10 p. 2149 - 2151