2,4,6-三苯基三嗪合成路线 （共 216 条）
反应条件
T=250°C; 0.166667 h;
参考文献
Cook, Lawrence S.; Prudhoe, Gordon; Venayak, Narinder D.; Wakefield, Basil J.
Journal of Chemical Research, Miniprint, 1982 , # 5 p. 1357 - 1367
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 5 min, 2.) THF, hexane, -78 deg C to r.t., 12 h; r.t., 27 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Buhmann, Martin; Moeller, Manfred H.; Rodewald, Ute; Wuerthwein, Ernst-Ulrich
Angewandte Chemie, 1994 , vol. 106, # 22 p. 2386 - 2389
反应条件
in tetrahydrofuran conventional Schlenk technique; PhCN added with stirring to NdI2; 5 min;PhCN removed in vac.; THF added; pptd. for 1 h; decanted; solvent remov ed from mother liquor; MeOH added; pptd. (20°C, 20 h); MeOH removed from soln.; pptd. by adding H2O; ppt. after decantation washed with cold THF, dried in vac. (NdI3(thf)3);ppt. after H2O addition sepd. by centrifuging, dried (NdI(OH)2(H2O)5); elem. anal.;
参考文献
Balashova; Khoroshenkov; Kusyaev; Eremenko; Aleksandrov; Fukin; Bochkarev
Russian Chemical Bulletin, 2004 , vol. 53, # 4 p. 825 - 829
反应条件
sulfur nitride; oxygen in toluene 24 h; Heatingpresence of p-hydroquinone; m-dinitrobenzene; Product distribution;
参考文献
Mataka, Shuntaro; Hosoki, Akira; Takahashi, Kazufumi; Tashiro, Masashi
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1681 - 1685
反应条件
2,4,6-trimethyl-pyridine; lithium; carbonic acid diethyl ester 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
参考文献
Figeys, H. P.; Mathy, A.
Tetrahedron Letters, 1981 , vol. 22, # 15 p. 1393 - 1396
反应条件
N,n-dimethyl-p-chloro-benzamide T=200°C; 6 h; different reagents; Product distribution;
参考文献
Schroth, Werner; Kluge, Helmut
Zeitschrift fuer Chemie (Stuttgart, Germany), 1986 , vol. 26, # 8 p. 295 - 297
参考文献
Fireman
Journal of the American Chemical Society, 1930 , vol. 52, p. 2951
反应条件
lithium; benzonitrile 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
反应条件
lithium; benzonitrile 1.) diethyl ether, reflux, 1 h, 2.) ether, reflux, 2.5 h, 3.) ether; Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Compagnon, Paul-Louis; Gasquez, Francoise; Kimny, Tan
Bulletin des Societes Chimiques Belges, 1986 , vol. 95, # 1 p. 57 - 64
