2,4,6-三苯基三嗪合成路线 (共 216 条)
反应条件
ammonia; iodine T=-39°C;
参考文献
Strain
Journal of the American Chemical Society, 1927 , vol. 49, p. 1568
反应条件
in benzene T=80°C; 0.25 h;
参考文献
Borovikova, G. S.; Levchenko, E. S.; Borovik, E. I.; Darmokhval, E. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 171 - 176
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 190 - 196
反应条件
in benzene T=80°C; 0.25 h;
参考文献
Borovikova, G. S.; Levchenko, E. S.; Borovik, E. I.; Darmokhval, E. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 171 - 176
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 190 - 196
反应条件
1: 1,2,3,4-tetrapropyl-1,4-diiodo-1,3-diene With tert.-butyl lithium in diethyl ether; pentane T=-78°C; 1 h; Inert atmosphere; 2: With N,N,N',N',N'',N''-hexamethylphosphoric triamide in diethyl ether; pentane T=20°C; 0.5 h; Inert atmosphere; 3: benzonitrile in diethyl ether; pentane T=20°C; 3 h; Inert atmosphere;
参考文献
Yu, Nan; Wang, Congyang; Zhao, Fei; Liu, Lantao; Zhang, Wen-Xiong; Xi, Zhenfeng
Chemistry - A European Journal, 2008 , vol. 14, # 18 p. 5670 - 5679
反应条件
1: With Au/Al2O3; ammonia; oxygen in toluene T=150°C; P=10126 Torr; 23 h; Autoclave; 2: in toluene T=100°C; 24 h; Inert atmosphereAutoclave;
参考文献
Ishida, Tamao; Watanabe, Hiroto; Takei, Takashi; Hamasaki, Akiyuki; Tokunaga, Makoto; Haruta, Masatake
Applied Catalysis A: General, 2012 , vol. 425-426, p. 85 - 90
反应条件
ammonium acetate; oxygen in methanol 5 h; Ambient temperature;
参考文献
Panda; Patro, Balaram; Padhy
Journal of the Indian Chemical Society, 1996 , vol. 73, # 6 p. 283 - 284
反应条件
trifluorormethanesulfonic acid in nitromethane T=100°C; 6 h; Yield given;
参考文献
El-Khagawa, Ahmed M.
Bulletin de la Societe Chimique de France, 1987 , # 2 p. 372 - 374
反应条件
samarium diiodide T=55°C; 15 h;
参考文献
Xu, Fan; Sun, Jianhua; Shen, Qi
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1867 - 1869
反应条件
iodine; sodium carbonate; benzene
参考文献
Strain
Journal of the American Chemical Society, 1927 , vol. 49, p. 1568
反应条件
ammonium hydroxide; Fremy’s salt in pyridine 192 h; Ambient temperature;
参考文献
Llobera, A.; Saa, J. M.; Peralta, A.
Synthesis, 1985 , # 1 p. 95 - 98