2,4,6-三苯基三嗪合成路线 (共 216 条)
反应条件
n-butyllithium in diethyl ether T=20°C; 6 h; Further byproducts given;
参考文献
Cook, Lawrence S.; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2392 - 2397
反应条件
N,n-dimethyl-p-chloro-benzamide T=200°C; 6 h;
参考文献
Schroth, Werner; Kluge, Helmut
Zeitschrift fuer Chemie (Stuttgart, Germany), 1986 , vol. 26, # 8 p. 295 - 297
反应条件
in cyclohexane Irradiation;
参考文献
Pavlik, James W.; Changtong, Chuchawin; Vikki
Journal of Organic Chemistry, 2003 , vol. 68, # 12 p. 4855 - 4861
反应条件
1: 93 percent / tert-butyl hypochlorite / benzene / 24 h / 20 °C 2: SOCl2 / 4 h / 70 - 80 °C View Scheme
参考文献
Borovikova, G. S.; Levchenko, E. S.; Borovik, E. I.; Darmokhval, E. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 171 - 176
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 190 - 196
反应条件
1: 1.) hydrazine hydrate; 2.)sodium nitrite / 1.) room t., 48h; 2.) acetic acid, 0 deg C 2: 6 percent Turnov. / toluene / Heating View Scheme
参考文献
Figeys, H. P.; Mathy, A.
Tetrahedron Letters, 1981 , vol. 22, # 15 p. 1393 - 1396
反应条件
1: benzene 2: toluene 3: KCN / benzonitrile View Scheme
参考文献
Johnson, David K.; Rukachaisirikul, Thitima; Sun, Yan; Taylor, Nicholas J.; Canty, Allan J.; Carty, Arthur J.
Inorganic Chemistry, 1993 , vol. 32, p. 5544 - 5552
反应条件
sodium hydride in ethylene glycol dimethyl ether 40 h; Ambient temperature;
参考文献
Lorente, Antonio; Gamez, Pedro; Mar Contreras, Maria del
Heterocycles, 1994 , vol. 38, # 1 p. 113 - 124
反应条件
thionyl chloride T=70 - 80°C; 4 h; Yield given;
参考文献
Borovikova, G. S.; Levchenko, E. S.; Borovik, E. I.; Darmokhval, E. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 171 - 176
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 190 - 196
反应条件
water; oxygen; nickel T=195°C; 50 h;
参考文献
Eisch, John J.; Ma, Xin; Han, Kyoung I.; Gitua, John N.; Krueger, Carl
European Journal of Inorganic Chemistry, 2001 , # 1 p. 77 - 88
反应条件
1: 43 percent / BF3*OEt2 / CHCl3 / 4 h / 20 °C 2: 96 percent / mCPBA; NaHCO3 / CHCl3 / 1 h / 0 °C 3: 12 percent / BF3*OEt2 / CHCl3 / 2 h / 20 °C View Scheme
参考文献
Shibuya, Isao
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 11 p. 3369 - 3370