(2-氧代环戊基)-乙酸甲酯合成路线 （共 13 条）
参考文献
Cooper, Kelvin; Pattenden, Gerald
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 799 - 809
反应条件
1: TsOH / benzene / 2 h / Heating
2: KOH / methanol / 10 h / Ambient temperature
3: 1.) Im2CO 3.) TsN3, Et3N / 1.) THF, room temp., 0.5 h; 2.) THF, room temp., 15 h; 3.) CH3CN, room temp., 2 h
4: 5percent Rh2(OAc)4 / CH2Cl2 / 1 h / 20 °C
5: NaBH4 / methanol / 1 h / -50 °C
6: Et3N / CH2Cl2 / 0.5 h / -20 °C
7: DBU / benzene / 4 h / 10 °C
View Scheme
参考文献
Hashimoto, Shun-ichi; Shinoda, Tomohiro; Shimada, Yasunaga; Honda, Takeshi; Ikegami, Shiro
Tetrahedron Letters, 1987 , vol. 28, # 6 p. 637 - 640
反应条件
pyridinium p-toluenesulfonate in benzene
5 h; Heating;
参考文献
Reimann, Eberhard; Ettmayr, Christian; Polborn, Kurt
Monatshefte fur Chemie, 2004 , vol. 135, # 5 p. 557 - 579
