反应条件
1: NaH / 1.) DMF, RT, 2 h, 2.) 100-110 deg C, 2.5 h 2: 50 percent / conc. HCl / 96 h / Heating 3: 75 percent / LiAlH4, 2-Propanol / diethyl ether / 3 h / -60 - -50 °C / Other temperatures, other reaction times, different reactant ratios View Scheme
参考文献
Tsuboi, Sadao; Shimozuma, Kazuo; Takeda, Akira
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1517 - 1520