4-[(二甲基氨基)亚甲基]-3-甲基-1-苯基-2-吡唑啉-5-酮合成路线 (共 4 条)
反应条件
oxygen in N,N-dimethyl acetamide T=80 - 90°C; 8 h;
参考文献
Smirnova, N. P.; Kvitko, I. Ya.; El'tsov, A. V.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 582 - 590
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 3 p. 650 - 660
反应条件
in anhydrous xylene
6 h; Reflux;
参考文献
Abdel-Megid
Chemistry of Heterocyclic Compounds, 2010 , vol. 46, # 3 p. 316 - 324
反应条件
trichlorophosphate
3 h; Heating;
参考文献
Shemarova; Maizel; Voznyi; Stepanova; Khovanskikh
Pharmaceutical Chemistry Journal, 2000 , vol. 34, # 10 p. 530 - 532
反应条件
in methanol
5 h; Ambient temperature;
参考文献
Koelle, Ulrich; Kolb, Bernd; Mannschreck, Albrecht
Chemische Berichte, 1980 , vol. 113, # 7 p. 2545 - 2565