1: octadecan-1-yne; trimethylaluminum With zirconocene dichloride in dichloromethane; toluene
T=0 - 20°C;
2: With n-butyllithium in hexane
0.25 h;
3: formaldehyd in tetrahydrofuran; hexane
参考文献
Dai, Peng; Trullinger, Tony K.; Liu, Xuejun; Dussault, Patrick H.
Journal of Organic Chemistry, 2006 , vol. 71, # 6 p. 2283 - 2292
