1-苯基-2-丁烯-1-酮合成路线 (共 117 条)
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-30°C; 24 h;
参考文献
Ochiai, Masahito; Yoshimura, Akira; Mori, Takeshi; Nishi, Yoshio; Hirobe, Masaya
Journal of the American Chemical Society, 2008 , vol. 130, # 12 p. 3742 - 3743
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; ethylene,methyl acetate; carbon monoxide
参考文献
Kondo, Teruyuki; Kodoi, Kouichi; Nishinaga, Eiji; Okada, Takumi; Morisaki, Yasuhiro; Watanabe, Yoshihisa; Mitsudo, Take-Aki
Journal of the American Chemical Society, 1998 , vol. 120, # 22 p. 5587 - 5588
反应条件
pyridine; dihydrogen peroxide in dichloromethane T=0 - 20°C; 0.5 h;
参考文献
Patra, Pranab K.; Shanmugasundaram, Kandasamy; Matoba, Manabu; Nishide, Kiyoharu; Kajimoto, Tetsuya; Node, Manabu
Synthesis, 2005 , # 3 art. no. F12504SS, p. 447 - 457
反应条件
tetrakis(triphenylphosphine) palladium(0); tris(4-methylphenyl)-phosphine in 1,4-dioxane T=100°C; 12 h; Inert atmosphere;
参考文献
Manjolinho, Filipe; Gruenberg, Matthias F.; Rodriguez, Nuria; Goossen, Lukas J.
European Journal of Organic Chemistry, 2012 , # 25 p. 4680 - 4683
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; ethylene,methyl acetate; carbon monoxide in tetrahydrofuran
参考文献
Kondo, Teruyuki; Kodoi, Kouichi; Nishinaga, Eiji; Okada, Takumi; Morisaki, Yasuhiro; Watanabe, Yoshihisa; Mitsudo, Take-Aki
Journal of the American Chemical Society, 1998 , vol. 120, # 22 p. 5587 - 5588
反应条件
1: With 4 A molecular sieve; (S)-(minus;)-1,1'-bi-2-naphthol; zirconium tetra-t-butoxide in toluene T=-20°C; 3 h; 2: With tert-butyl methyl ether in toluene T=0°C; Oppenauer oxidation; 24 h;
参考文献
Kurosu, Michio; Lorca, Miguel
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1765 - 1769
反应条件
aluminum oxide in diethyl ether 2 h;
参考文献
Kurono, Nobuhito; Nii, Noriyuki; Sakaguchi, Yusuke; Uemura, Masato; Ohkuma, Takeshi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 24 p. 5541 - 5544
反应条件
diallyl carbonate; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane in acetonitrile 1 h; Heating;
参考文献
Tsuji, Jiro; Minami, Ichiro; Shimizu, Isao
Tetrahedron Letters, 1983 , vol. 24, # 50 p. 5635 - 5638
反应条件
palladium diacetate; oxygen in dimethyl sulfoxide T=25°C; 72 h;
参考文献
Larock, Richard C.; Hightower, Timothy R.; Kraus, George A.; Hahn, Pat; Zheng, Deye
Tetrahedron Letters, 1995 , vol. 36, # 14 p. 2423 - 2426
反应条件
C2H6S*C18H15OP*Cl3ORe in ethylene glycol dimethyl ether T=80°C; Meyer-Schuster rearrangement; 24 h;
参考文献
Stefanoni, Massimo; Luparia, Marco; Porta, Alessio; Zanoni, Giuseppe; Vidari, Giovanni
Chemistry - A European Journal, 2009 , vol. 15, # 16 p. 3940 - 3944