1-苯基-2-丁烯-1-酮合成路线 (共 117 条)
反应条件
triethylamine; palladium on activated charcoal in toluene T=200°C; 12 h;
参考文献
Coquerel, Yoann; Bremond, Paul; Rodriguez, Jean
Journal of Organometallic Chemistry, 2007 , vol. 692, # 22 p. 4805 - 4808
反应条件
1: nBuLi, TMEDA / diethyl ether; hexane 2: CrO3 / diethyl ether; H2O View Scheme
参考文献
Rautenstrauch,V. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 2576 - 2580
反应条件
1: KOtBu / dimethylsulfoxide 2: nBuLi, TMEDA / diethyl ether; hexane 3: CrO3 / diethyl ether; H2O View Scheme
参考文献
Rautenstrauch,V. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 2576 - 2580
反应条件
MoVIO2(acetylacetone)2; [(PPh3)AuCl]; silver trifluoromethanesulfonate in toluene T=20°C; Meyer-Schuster rearrangement; 1 h;
参考文献
Egi, Masahiro; Yamaguchi, Yoshiko; Fujiwara, Noboru; Akai, Shuji
Organic Letters, 2008 , vol. 10, # 9 p. 1867 - 1870
反应条件
aluminium trichloride in 1,2-dichloro-benzene 5 h; Heating;
参考文献
Yin, Wei; Ma, Yuan; Xu, Jiaxi; Zhao, Yufen
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4312 - 4315
反应条件
titanium tetrachloride in dichloromethane T=-70°C; 1 h;
参考文献
Mulzer, Johann; Bruentrup, Gisela; Hartz, Georg; Kuehl, Uwe; Blaschek, Ursula; Boehrer, Gerald
Chemische Berichte, 1981 , vol. 114, # 11 p. 3701 - 3724
反应条件
nickel in ethylene glycol dimethyl ether T=85°C; 0.5 h;
参考文献
Inaba, Shin-ichi; Rieke, Reuben D.
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1373 - 1381
反应条件
palladium (II) trifluoroacetate in tetrahydrofuran T=70°C; 8 h;
参考文献
Obora, Yasushi; Nakanishi, Masafumi; Tokunaga, Makoto; Tsuji, Yasushi
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5835 - 5837
反应条件
1: in tetrahydrofuran T=0°C; 0.5 h; 2: With dipyridinium dichromate in N,N-dimethyl-formamide T=20°C; 1 h; Further stages.;
参考文献
Huang, Xian; Xie, Meihua
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 8895 - 8900
反应条件
tris (triphenylphosphine)rhodium(I) chloride in toluene T=80°C; 3 h; Inert atmosphere; optical yield given as percent de;
参考文献
Kashiwabara, Taigo; Tanaka, Masato
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3958 - 3961