1-苯基-2-丁烯-1-酮合成路线 （共 117 条）
反应条件
1: zinc / N,N-dimethyl-formamide / Inert atmosphere 2: Jone's reagent 3: aluminum oxide / acetone / 2 h View Scheme
参考文献
Zhuo, Lian-Gang; Yao, Zhong-Ke; Yu, Zhi-Xiang
Organic Letters, 2013 , vol. 15, # 18 p. 4634 - 4637
反应条件
1: tetrahydrofuran; Bu2O / 1 h / 0 °C 2: manganese(IV) oxide / diethyl ether / 24 h / 20 °C View Scheme
参考文献
Wu, Dan; O'Shea, Donal F.
Organic Letters, 2013 , vol. 15, # 13 p. 3392 - 3395
反应条件
samarium diiodide in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Zhang, Yongmin; Liu, Tianchun; Lin, Ronghui
Synthetic Communications, 1988 , vol. 18, # 16-17 p. 2003 - 2010
反应条件
1: 1.) triethylamine / 1.) toluene, 0 deg C, 15 min. 2.) 25 deg C, 16 h 2: 76 percent / B(OH)3, H2 / Raney nickel / methanol; H2O / 2.5 h 3: 99 percent / BF3*O(C2H5)2 / CH2Cl2 / 1 h / 0 °C 4: silica gel View Scheme
参考文献
Curran, Dennis P.; Kim, Byeang Hyean
Synthesis, 1986 , # 4 p. 312 - 315
反应条件
1: 76 percent / B(OH)3, H2 / Raney nickel / methanol; H2O / 2.5 h 2: 99 percent / BF3*O(C2H5)2 / CH2Cl2 / 1 h / 0 °C 3: silica gel View Scheme
参考文献
Curran, Dennis P.; Kim, Byeang Hyean
Synthesis, 1986 , # 4 p. 312 - 315
反应条件
1-ethyl-piperidine; dichloro bis(acetonitrile) palladium(II); tin(II) trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine 1.) methylene chloride, 0 deg C, 15 min; 2.) methylene chloride, RT; different ketones and acid captors; Product distribution;
参考文献
Engman Lars
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4031 - 4037
反应条件
lithium chloride in tetrahydrofuran
参考文献
Dieter, R. Karl; Sharma, Ram R.; Yu, Huayun; Gore, Vinayak K.
Tetrahedron, 2003 , vol. 59, # 7 p. 1083 - 1094
反应条件
sodium hydrogencarbonate in dichloromethane 4 h;
参考文献
Engman Lars
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4031 - 4037
反应条件
[RhCl(cis-cyclooctene)2]2; 1,3-bis-(diphenylphosphino)propane in toluene T=100°C; 2 h;
参考文献
Oguma, Kazuaki; Miura, Masahiro; Satoh, Tetsuya; Nomura, Masakatsu
Journal of Organometalic Chemistry, 2002 , vol. 648, # 1-2 p. 297 - 301
反应条件
1: diethyl ether; tetrahydrofuran / 0.5 h / 0 - 20 °C / |Inert atmosphere 2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.33 h / 20 °C 3: bis(1,1-diphenylphosphino)methane; tetracarbonylbis(μ-chloro)dirhodium(I) / ethylene glycol dimethyl ether / 20 h / 65 °C / |Inert atmosphere View Scheme
参考文献
Zhuo, Lian-Gang; Yao, Zhong-Ke; Yu, Zhi-Xiang
Organic Letters, 2013 , vol. 15, # 18 p. 4634 - 4637
