1-苯基-2-丁烯-1-酮合成路线 （共 117 条）
反应条件
1: acetonitrile / 3 h / 20 °C 2: sodium hydroxide / acetonitrile / 17 h / |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 5 p. 1427 - 1433
反应条件
aluminium trichloride
参考文献
Allen,J.M. et al.
Tetrahedron, 1977 , vol. 33, p. 2083 - 2087
参考文献
Plattner; Fuerst; Jirasek
Helvetica Chimica Acta, 1947 , vol. 30, p. 1320,1328
反应条件
1: arsenic acid; zinc-chloride; aqueous hydrochloric acid 2: Hydrogenation.Erhitzen des erhaltenen Amins mit 1-Phenyl-but-2-en-1-on, sirupoese H3PO4 und H3AsO4 View Scheme
参考文献
Case; Brennan
Journal of Organic Chemistry, 1954 , vol. 19, p. 919,921
反应条件
tri-n-butyl-tin hydride in benzene T=20 - 80°C; 3 h; Inert atmosphere;
参考文献
Krafft, Marie E.; Vidhani, Dinesh V.; Cran, John W.
Synlett, 2011 , # 16 art. no. S05311ST, p. 2355 - 2358
反应条件
water; Bu2SnIH; Ph2SiH2 in tetrahydrofuran T=20°C; Aldol reaction; 3 h; optical yield given as percent dediastereoselective reaction;
参考文献
Shibata, Ikuya; Tsunoi, Shinji; Sakabe, Kumiko; Miyamoto, Shinji; Kato, Hirofumi; Nakajima, Hideto; Yasuda, Makoto; Baba, Akio
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13335 - 13338
反应条件
1: 69 percent / 1.) -23 deg C, 5.25 h, 2.) room temperature, 45 min 2: 75 percent / Raney nickel / ethanol / 20 h / 90 °C 3: 88 percent / HBF4*Et2O / CH2Cl2 / 1 h / Ambient temperature 4: 70 percent / Et3N, MCPBA / diethyl ether / 2.25 h / Ambient temperature View Scheme
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
反应条件
acetone; palladium dichloride T=15.7°C; Hydrogenation;
参考文献
Straus; Grindel
Justus Liebigs Annalen der Chemie, 1924 , vol. 439, p. 303
参考文献
Straus; Grindel
Justus Liebigs Annalen der Chemie, 1924 , vol. 439, p. 303
反应条件
1,3,5-trimethylphenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=20°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Chen, Shaojin; Hao, Lin; Zhang, Yuexia; Tiwari, Bhoopendra; Chi, Yonggui Robin
Organic Letters, 2013 , vol. 15, # 22 p. 5822 - 5825
