Mochalov, S. S.; Fedotov, A. N.; Kupriyanova, E. A.; Shabarov, Yu. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 5 p. 559 - 564
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 5 p. 688 - 694
in tetrahydrofuran Nitrosobenzene soln. in THF under N2 is stirred at 25°C until it is light blue in color, to this soln. is added carbene complex in THF, the soln. is heated under reflux.; cooling of resulting olive green soln. to 25°C, solvent removal, residue is dissolved in CH2Cl2, filtn., solvent removal from orange filtrate, residue is dissolved in a 19:1 hexane:ethyl acetate soln., purifn. by chromy., three fractions;
参考文献
Herndon, James W.; McMullen, Leonard A.
Journal of Organometallic Chemistry, 1989 , vol. 368, p. 83 - 102
