sodium tetrahydroborate; antimony(III)tribromide in tetrahydrofuran; dimethyl sulfoxide T=0 - 22°C; var. ratio of reagents; other 2,3-dibromo1,4-butanediones, and α-bromo ketones; Product distribution;
1: Mn(II) stearate / 120 °C / |Inert atmosphere 2: Mn(OAc)3•2H2O / 110 °C / |Inert atmosphere View Scheme
参考文献
Bukharkina, Tatiana V.; Grechishkina, Olga S.; Digurov, Nikolai G.; Krukovskaya, Nadezhda V.
Organic Process Research and Development, 2003 , vol. 7, # 2 p. 148 - 154
