3-(2-羟基苯基)丙酸合成路线 （共 44 条）
反应条件
sodium tetrahydroborate; sodium hydroxide in water T=20 - 60°C;
参考文献
Rao, Gopal Krishna; Gowda, Narendra B.; Ramakrishna, Ramesha A.
Synthetic Communications, 2012 , vol. 42, # 6 p. 893 - 904
反应条件
hydrogen; palladium on activated charcoal in ethanol 1.5 h;
参考文献
Amsberry, Kent L.; Borchardt, Ronald T.
Journal of Organic Chemistry, 1990 , vol. 55, # 23 p. 5867 - 5877
反应条件
hydrogen; potassium hydroxide in water T=20°C; P=760.051 Torr; 0.5 h; Sealed tube;
参考文献
Lim, Minkyung; De Castro, Kathlia A.; Oh, Seungchan; Lee, Kangsuk; Chang, Young-Wook; Kim, Hokun; Rhee, Hakjune
Applied Organometallic Chemistry, 2011 , vol. 25, # 1 p. 1 - 8
反应条件
1: With water; sodium hydroxide in methanol 0.5 h; Reflux; 2: With hydrogenchloride in methanol; water pH=3;
参考文献
Marumoto, Shinsuke; Miyazawa, Mitsuo
Tetrahedron, 2011 , vol. 67, # 2 p. 495 - 500
反应条件
methanol; formic acid; water; silica gel; palladium dichloride 0.916667 h; Irradiationmicrowave;
参考文献
Kumar, Vinod; Sharma, Anuj; Sinha, Arun K.
Helvetica Chimica Acta, 2006 , vol. 89, # 3 p. 483 - 495
反应条件
1: 38 percent / oxone; NaHCO3; aq. Na2*EDTA / acetonitrile / 2 h / 20 °C 2: aq. KOH / 19 h / Heating View Scheme
参考文献
Yang, Dan; Wong, Man-Kin; Yan, Zheng
Journal of Organic Chemistry, 2000 , vol. 65, # 13 p. 4179 - 4184
反应条件
1: 0.72 g / pyridine / CH2Cl2 / 4 h / -10 °C 2: 38 percent / oxone; NaHCO3; aq. Na2*EDTA / acetonitrile / 2 h / 20 °C 3: aq. KOH / 19 h / Heating View Scheme
参考文献
Yang, Dan; Wong, Man-Kin; Yan, Zheng
Journal of Organic Chemistry, 2000 , vol. 65, # 13 p. 4179 - 4184
反应条件
1: oxalyl chloride / CH2Cl2 / 2 h / 20 °C 2: 0.72 g / pyridine / CH2Cl2 / 4 h / -10 °C 3: 38 percent / oxone; NaHCO3; aq. Na2*EDTA / acetonitrile / 2 h / 20 °C 4: aq. KOH / 19 h / Heating View Scheme
参考文献
Yang, Dan; Wong, Man-Kin; Yan, Zheng
Journal of Organic Chemistry, 2000 , vol. 65, # 13 p. 4179 - 4184
反应条件
sodium hydroxide T=245 - 250°C;
参考文献
Meyer; Beer; Lasch
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1670
Full Text Show Details
Kinzlberger and Co.
Patent: DE276667 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 562
反应条件
potassium hydroxide Hydrolysis; 19 h; Heating;
参考文献
Yang, Dan; Wong, Man-Kin; Yan, Zheng
Journal of Organic Chemistry, 2000 , vol. 65, # 13 p. 4179 - 4184
