3-甲基-4-硝基-1,2,5-恶二唑 2-氧化物合成路线 （共 4 条）
反应条件
1: With sodium nitrite in dimethyl sulfoxide
T=0 - 2°C; pH=4 - 5; 0.333333 h;
2: With hydrogenchloride in water; dimethyl sulfoxide
T=0 - 2°C; 2.5 h;
参考文献
Finogenov; Ovchinnikov; Kulikov; Makhova
Russian Chemical Bulletin, 2012 , vol. 61, # 2 p. 472 - 475
Izv. Akad. Nauk, Ser. Khim., 2012 , vol. 61, # 2 p. 469 - 472
反应条件
nitric acid in water
1.a) 50 deg C, b) 50 to 70 deg C, 2.) 70 deg C, 48 h; Yield given. Title compound not separated from byproducts;
参考文献
Gakh, A. A.; Ugrak, B. I.; Kiseleva, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.2. p. 1883 - 1888
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , vol. 39, # 9 p. 2069 - 2075
反应条件
dinitrogen tetraoxide
参考文献
Levy; Scaife
Journal of the Chemical Society, 1946 , p. 1100,1102, 1104
反应条件
dihydrogen peroxide
1) CH2Cl2, 0 deg C, 2) CH2Cl2, 20 deg C; Yield given. Multistep reaction;
参考文献
Rakitin, O. A.; Vlasova, O. G.; Chertanova, L. F.; Khmel'nitskii, L. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 7.2 p. 1474 - 1478
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 7 p. 1625 - 1629
