二(2,4,5-三甲基苯基)甲烷合成路线 （共 10 条）
反应条件
phosphorus; hydrogen iodide
T=200°C; im Rohr;
参考文献
Wenzel
Monatshefte fuer Chemie, 1914 , vol. 35, p. 948
反应条件
indium(III) chloride
T=120°C;
参考文献
Sun, Hong-Bin; Hua, Ruimao; Yin, Yingwu
Tetrahedron Letters, 2006 , vol. 47, # 14 p. 2291 - 2294
参考文献
Vavon; Bolle; Calin
Bulletin de la Societe Chimique de France, 1939 , vol. <5> 6, p. 1025,1033
反应条件
1: AlCl3
2: concentrated hydriodic acid; phosphorus / 200 °C / im Rohr
View Scheme
参考文献
Wenzel
Monatshefte fuer Chemie, 1914 , vol. 35, p. 948
反应条件
sulfuric acid; acetic acid
参考文献
Wenzel
Monatshefte fuer Chemie, 1914 , vol. 35, p. 948
反应条件
in dichloromethane
(electrolysis);
参考文献
Nyberg,K.
Acta Chemica Scandinavica (1947-1973), 1970 , vol. 24, p. 1609 - 1617
反应条件
toluene-4-sulfonic acid
参考文献
Hendrickson; Wadsworth
Industrial and Engineering Chemistry, 1958 , vol. 50, p. 877
反应条件
palladium diacetate in trifluoroacetic acid
T=90°C; 6 h; in presence of K4H<CoW12O40>; velocity related to benzene reactivity toward biaryl formation; MechanismRate constant;
参考文献
Kozhevnikov, Ivan V.; Kim, Vladimir I.; Talzi, Eugeni P.; Sidelnikov, Vladimir N.
Journal of the Chemical Society, Chemical Communications, 1985 , # 20 p. 1392 - 1394
反应条件
zinc(II) chloride; zinc
1.)70-80 deg C, 5 h 2.)AcOH, 3 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Pozdnyakovich, Yu. V.; Borodovitsyn, V. V.; Pozdnyakovich, S. A.; Shein, S. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 353 - 359
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 2 p. 403 - 411
参考文献
Shell Devel. Co.
Patent: US2819322 , 1953 ;
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Shell Devel. Co.
Patent: USREISSUE24579 , 1958 ;
