双(2-羟基甲基苯基)硫化物合成路线 （共 14 条）
反应条件
1: 280 °C / im Rohr
2: sulfuric acid
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参考文献
Hinsberg
Chemische Berichte, 1910 , vol. 43, p. 1875
反应条件
in diethyl ether
72 h; Ambient temperature;
参考文献
Hellwinkel, Dieter; Bohnet, Siegbert
Chemische Berichte, 1987 , vol. 120, p. 1151 - 1174
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether
T=20°C; 16 h;
2: With water; sodium sulfate in tetrahydrofuran; diethyl ether
Product distribution / selectivity;
参考文献
XENON PHARMACEUTICALS INC.
Patent: US2008/234384 A1, 2008 ;
Location in patent: Page/Page column 47 ;
反应条件
1: CrO3; glacial acetic acid
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参考文献
Mayer
Chemische Berichte, 1910 , vol. 43, p. 590
