1,3-二氢异苯并呋喃合成路线 (共 101 条)
反应条件
1: 80 percent / lithium aluminum hydride / diethyl ether / 1 h / Heating 2: 63 percent / PCC 3: 79 percent / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 4: 0.2 M NaOCH3 / methanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
1: 68 percent / sodium hydroxide / aq. ethanol / 10 h / Heating 2: 80 percent / lithium aluminum hydride / diethyl ether / 1 h / Heating 3: 63 percent / PCC 4: 79 percent / 1.) 60 deg C, 3 h, 2.) room temp., 3 h, 3.) -20 deg C, overnight 5: 0.2 M NaOCH3 / methanol / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
zirconium oxide in isopropyl alcohol T=320°C; other lactone;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 1 p. 262 - 266
反应条件
tris (triphenylphosphine)rhodium(I) chloride in ethanol T=25°C; 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1357 - 1364
反应条件
(tributylphosphoranylidene)acetonitrile in tetrahydrofuran; toluene T=80°C; Mitsunobu reaction; 2.5 h; Inert atmosphere;
参考文献
Heterocycles, , vol. 85, # 7 p. 1711 - 1720
反应条件
1,4-dioxane; copper oxide-chromium oxide T=330°C; P=88260.9 Torr; Hydrogenation;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 233, p. 1124
反应条件
potassium tert-butylate in tert-butyl alcohol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
sodium ethanolate in ethanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473
反应条件
sodium methylate in methanol 2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 111, # 4 p. 1465 - 1473