反应条件
1.1: triethylamine / N,N-dimethyl-formamide / 20 - 50 °C 1.2: 6 h / 100 °C 2.1: trichlorophosphate / 0.67 h / cooling with ice 2.2: 3 h / 20 °C 2.3: 0.5 h 3.1: ammonium acetate / 1 h / Reflux 4.1: ethanol; sodium tetrahydroborate / tetrahydrofuran / 1.5 h / 20 °C / cooling with ice 4.2: 1 h / pH 4 5.1: trichlorophosphate / 0.83 h / cooling with ice 5.2: 2.58 h / 50 °C 6.1: hydroxylamine hydrochloride; pyridine / tetrahydrofuran / 1 h / 50 °C 6.2: 3.5 h / 50 °C / Reflux 7.1: hydrogen / palladium 10 on activated carbon / methanol / 1 h / 40 °C / 750.08 Torr 8.1: water; acetone / 3.25 h / 20 °C / Reflux 9.1: sodium carbonate / water / pH 8 - 9 10.1: sodium carbonate / ethanol; tert-butyl alcohol / 42 h / 50 - 90 °C 11.1: sodium hydroxide; water / methanol / 1.25 h / 20 °C / cooling with ice 12.1: sodium hydroxide; dihydrogen peroxide / water; dimethyl sulfoxide / 2.25 h / 20 - 25 °C View Scheme
参考文献
Yan, Pu-Cha; Zhang, Xian-Yi; Hu, Xiao-Wei; Zhang, Bin; Zhang, Xiang-Dong; Zhao, Michael; Che, Da-Qing; Li, Yuan-Qiang; Zhou, Qi-Lin
Tetrahedron Letters, 2013 , vol. 54, # 11 p. 1449 - 1451
