1: 99 percent / NaBH(OAc)3 / acetic acid / 1 h / 20 °C
2: 88 percent / DDQ / tetrahydrofuran / 0.75 h / 0 - 5 °C
3: 70 percent / TFA / ethyl acetate / 12 h / 60 °C
4: 49 percent / K2CO3 / dimethylformamide / 20 °C
View Scheme
参考文献
Faul, Margaret M.; Grutsch, John L.; Kobierski, Michael E.; Kopach, Michael E.; Krumrich, Christine A.; Staszak, Michael A.; Udodong, Uko; Vicenzi, Jeffrey T.; Sullivan, Kevin A.
Tetrahedron, 2003 , vol. 59, # 36 p. 7215 - 7229
1: 99 percent / NaBH(OAc)3 / acetic acid / 1 h / 20 °C
2: 88 percent / DDQ / tetrahydrofuran / 0.75 h / 0 - 5 °C
3: 70 percent / TFA / ethyl acetate / 12 h / 60 °C
View Scheme
参考文献
Faul, Margaret M.; Grutsch, John L.; Kobierski, Michael E.; Kopach, Michael E.; Krumrich, Christine A.; Staszak, Michael A.; Udodong, Uko; Vicenzi, Jeffrey T.; Sullivan, Kevin A.
Tetrahedron, 2003 , vol. 59, # 36 p. 7215 - 7229
1: Bi(NO3)3·5H2O / dichloromethane / 1 h / 20 °C
2: manganese(IV) oxide / dichloromethane / 12 h / 20 °C
3: manganese(IV) oxide; water / dichloromethane / 2 h / 20 °C
View Scheme
